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Synthesis and Characterization Some of Metals (ƖƖ) Complexes' with Mixed Ligands of saccharinate and Isatin Schiff Base | ||
| Tikrit Journal of Pure Science | ||
| Article 1, Volume 22, Issue 6, 2017, Pages 56-64 | ||
| Authors | ||
| Anfal S. Ali; Ahmad Najem Abd; Modher Y. Mohammed | ||
| Abstract | ||
| This research paper includes synthesis and characterization of some complexes of Zn(II),Hg(II), Cd(II), Cu(II), Co(II), Ni(II) with mix ligands of saccharinate and Schiff base derived from Isatin. All the synthesized complexes have been characterized by elemental analysis, molar conductance, uv-visible, magnetic susceptibility, atomic absorption , infrared and 1H NMR spectroscopy ,Metal to ligand [M:L] ratio was obtained for all complexes in ethanol. The concluded chemical formulas of the complexes were [M(sac)2(L)2] ,where {M=(Zn(II) , Hg(II) ,Cd(II)} tetrahedral geometry and for the complexes [M(sac)2(L)(H2O)2] ,where (M=Co , Ni and Cu), were octahedral geometry, sac=saccharinate, and L=C14H10N2O2 | ||
| Keywords | ||
| Schiff Base; isatin; saccharin; complexes | ||
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