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Synthesis of azo- Schiff base and azo-oxazepine compounds from nucleus of 2,6-diaminopyridine by using Microwave Irradiation | ||
| Kirkuk Journal of Science | ||
| Article 1, Volume 12, Issue 1, 2017, Pages 435-446 PDF (0 K) | ||
| Document Type: Research Paper | ||
| DOI: 10.32894/kujss.2017.129730 | ||
| Authors | ||
| Ahmed Mousa Al-salami1; Nihad Ismael Al-khafaf2; Ahmood Khalaf Al-Jaboure1 | ||
| 1Tikrit university/ College of Science-Chemistry Dept | ||
| 2Kirkuk University/ College of Science - chemistry Dept | ||
| Abstract | ||
| Some new azo-schiff bases were prepared by reacting aromatic diazonium salts with aromatic Schiff bases .azo-oxazepine was prepared from the latter comounds via cycloaddition reaction with maleic anhydride using the enviorement friendly microwave technique as a participation to the applications of green chemistry .Spectroscopic methods (IR, 1HNMR) as well as some physical properties were used for the structural elucidation of the prepared compounds | ||
| Keywords | ||
| diaminopyridine; Azo; Schiff base; oxazepine; Microwave irradiation | ||
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