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Synthesis and Characterization of 1,2,3- Triazole Derivatives from D-Mannitol | ||
| Tikrit Journal of Pure Science | ||
| Article 1, Volume 22, Issue 9, 2017, Pages 58-68 | ||
| Author | ||
| Ihmood Kh. Juber | ||
| Abstract | ||
| This research included the use of azido D-Mannitol (3) to synthesize 1,2,3 triazole derivatives. Azido D – Mannitol (3) itself used as an intermediate which was prepared from reaction of 1, 2:5, 6-Di-o-isopropylidene-3,4-di-p-tosyl-D-Mannitol (2) with sodium azide. The prepared compound (3) was allowed to react with alkenes for the formation of corresponding 1,2,3 triazole (4a-e ). The structures of some prepared compounds were confirmed by physical properties and spectroscopic methods FT-IR , 1H-NMR , 13C-NMR and Mass spectra in addition to use TLC. | ||
| Keywords | ||
| Mannitol; Triazole; azide; isopropylidene | ||
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