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Preparation and Characterization of Derivatives of Pyrimidines in two ways Clascical and Microwave | ||
| Journal of University of Anbar for Pure Science | ||
| Article 6, Volume 10, Issue 3, 2016, Pages 22-34 PDF (799.32 K) | ||
| Document Type: Research Paper | ||
| DOI: 10.37652/juaps.2016.135152 | ||
| Authors | ||
| Waleed AL-Hiti* 1; Samea J.Khammase2; Bushra T.Mahdi3 | ||
| 1University Of Anbar- College of Education for Women | ||
| 2University of Baghdad - College of Science for Women | ||
| 3University Of Anbar- College of Education for Women. | ||
| Abstract | ||
| This study includes synthesis and characterization of new pyrimidine derivatives (R or Ar-2,3,4,6,7,8-hexahydroquinazolin-5(1H)-one), via of the reaction from cyclohexane-1,3-dione with aldehyde derivatives and guanidinehydrochlorid. Usingabsolute ethanol as a solvent .This mixture was refluxed for (4 – 6) hrs;While maintaining the pH at 6. The same derivatives of pyrimidine were prepared in microwave waytechnique.The prepared compounds were characterized by melting point , FT-IR , UV-Vis 1H-NMR and 13C-NMR spectroscopy | ||
| Keywords | ||
| preparation; Characterization; derivatives; Pyrimidines; Clascical; Microwave | ||
| References | ||
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