Amer Sallal, Z., Thamer Ghanem, H. (2018). Synthesis and Identification of New Oxazepine Derivatives bearing Azo group in their structures. , 59(1), 1-8.
Zainab Amer Sallal; Hasan Thamer Ghanem. "Synthesis and Identification of New Oxazepine Derivatives bearing Azo group in their structures". , 59, 1, 2018, 1-8.
Amer Sallal, Z., Thamer Ghanem, H. (2018). 'Synthesis and Identification of New Oxazepine Derivatives bearing Azo group in their structures', , 59(1), pp. 1-8.
Amer Sallal, Z., Thamer Ghanem, H. Synthesis and Identification of New Oxazepine Derivatives bearing Azo group in their structures. , 2018; 59(1): 1-8.

Synthesis and Identification of New Oxazepine Derivatives bearing Azo group in their structures

Iraqi Journal of Science
Article 1, Volume 59, Issue 1, 2018, Pages 1-8
Authors
Zainab Amer Sallal; Hasan Thamer Ghanem
Abstract
In this contribution new oxazepine compounds containing azo group were preppared. In the firststep,4-(dimethylamino)-3-((4-methoxy phenyl) diazenyl) benzaldehyde [Z] was synthesised by using 4-methoxyaniline. The second step was the condensation reaction between aldehyde group of the azo compound [Z] and different primary aromatic amines [4-hydroxyaniline, 4-chloroaniline and 4-amino-N-(pyrimidin-2-yl) benzenesulfonamide] to yield new azo Schiff bases compounds [A1-A3] respectively. In the final step, oxazepine compounds [B1-B3] and [B4-B6] were prepared from reaction imines compounds [A1-A3] with maleic anhydride and phathalic anhydride in dry benzene respectively. All these derivatives were characterized by melting points and FTIR spectroscopy, some of them were characterized by 1H-NMR spectroscopy.
Keywords
Azo compound; Schiff Base; oxazpines
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