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Synthesis and Characterization of Some New Metals Complexes of [N-( 4-chlorobenzoyl amino )-thioxomethyl] Anthranilic Acid (CBA) | ||
| journal of al-qadisiyah for pure science(quarterly) | ||
| Article 1, Volume 14, Issue 4, 2014, Pages 150-165 PDF (0 K) | ||
| Author | ||
| Abstract | ||
| A new ligand [N-(4-chloro benzoyl amino)-thioxo methyl] anthranilic acid (CBA) was synthesized by reaction of 4chlorobenzoyl isothiocyanate with anthranilic acid by using acetone as a solvent , The ligand was characterized by elemental analysis ,FT-IR,and13C, 1H-NMR spectra, some transition metals complexes of this ligand was prepared and characterized by FT-IR, UV-Visible spectra , conductivity measurements , magnetic susceptibility , atomic absorption and molar ratio ( M : L ). From results obtained ,the following formula [ M (CBA )2 ] where M+2 = Mn, Co , Ni , Cu , Pd , Zn , Cd ,and Hg , the proposed molecular structure for these complexes as tetrahedral geometry except copper and palladium complexes are have square planer geometry . | ||
| Keywords | ||
| anthranilic acid; chloro benzoyl isothiocyanate; complexes | ||
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