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Synthesis and Characterization of Magnetite Nanoparticles and the Effect of [Fe(sac)2(H2O)4].2H2O complex on its magnetic properties | ||
| Kirkuk Journal of Science | ||
| Article 1, Volume 14, Issue 1, 2019, Pages 86-96 PDF (1010.01 K) | ||
| Document Type: Research Paper | ||
| DOI: 10.32894/kujss.2019.14.1.7 | ||
| Authors | ||
| Ahmed Raoof* 1; Mustafa A. Alheety2; Luma Jassim2; Anwar Adil2 | ||
| 1Department of Medical Laboratory Technology, Imam Jaafar Al-Sadiq University, Kirkuk, Iraq. | ||
| 2Department of Chemistry, College of Science, University of Tikrit, Tikrit, Iraq. | ||
| Abstract | ||
| A novel inorganic complex (shell)@metal oxide (core) was demonstrated by simple and highly efficient synthesis of Fe3O4 nanoparticles (Fe3O4NPs) coated by [Fe(sac)2(H2O)4] .2H2O complex through one-pot reaction of prepared Fe3O4 nanoparticles and [Fe(sac)2(H2O)4].2H2O. The Fe3O4 NPs structure was characterized by infrared spectroscopy (IR), scanning electron microscope (SEM) and energy dispersive X-rays (EDX) while the resulted [Fe(sac)4(H2O)2]@Fe3O4NPs was characterized using IR spectroscopy and XRD. The magnetic feature, which is one of physical properties of Fe3O4NPs and the newly synthesized core-shell [Fe(sac)2(H2O)4]@Fe3O4NPs were examined in order to study how the Fe in its complex effects on the magnetic properties of magnetite nanoparticles. . | ||
| Keywords | ||
| Inorganic complex; NPs; sac; O complex; Magnetic properties | ||
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