preparation of palladium Catalyst from bauxite ore and using for kerosene treatment

Saeed, Wafa; Salim, Qaidar

doi:10.33899/edusj.2020.127951.1103

	preparation of palladium Catalyst from bauxite ore and using for kerosene treatment
Journal of Education and Science
Article 24, Volume 30, Issue 1, 2021, Pages 126-140 PDF (819.98 K)
Document Type: Research Paper
DOI: 10.33899/edusj.2020.127951.1103
Authors
Wafa Saeed^* ¹; Qaidar Salim²
¹Ministry of Education Nineveh Education Direstorate
²Department of Chemistry College of Education for Pure Science
Abstract
The research was aimed to used bauxite ore that has a high aluminum minerals which available in Al-Hussainiyat near al-Anbar district as a source of alumina which it used as a catalyst support after being loaded with palladium metal , The components of both bauxite ore and prepared catalyst were studied by X-ray diffraction and fluorescence as well as thermogravimetric analysis (TGA) of the prepared catalyst , After this the catalyst was used in the treatment of kerosene which is distilled at (150-260C0) under different conditions of the (temperature , reaction time and the ratio of catalyst) to know the optimal reaction conditions that determid by measuring the (FTIR) and chemical analysis. The optimal conditions: temperature was (250C0), reaction time was (2hours) and the catalyst ratio was (2%) .The catalyst appeard the ability to dehydrogenation reaction and reforming to form olefinic and aromatic compounds. The research also included the study of n-paraffins separated from kerosene samples that were treating in different temperatures (150,200,250C0 ) using (1HNMR).The results showed the ability of the catalyst towards catalytic cracking and converting n-paraffins to iso-paraffins
Keywords
kerosene,,; ,،,؛palladium,,; ,،,؛catalysts,,; ,،,؛alpha alumina

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