- All Journals
- Al-Qadisiyah University
- Basrah University
- Kirkuk University
- Mosul University
- The Iraqi Borad for Medical Specialization
- University of Anbar
- University of Technology
- Al Mustafa University
- Al-Zahraa University for Women
- Alnoor University
- Kunooz University
- Misan University
- Ninevah University
- Tikrit University
- University of Al-Hamdaniya
- University of Kerbala
Extraction and Analysis of Washington tree seed oil and Kulgan (Silybum marianum) seed oil | ||
| Journal of University of Anbar for Pure Science | ||
| Article 15, Volume 12, Issue 1, 2018, Pages 72-80 PDF (716.2 K) | ||
| Document Type: Research Paper | ||
| DOI: 10.37652/juaps.2022.171576 | ||
| Authors | ||
| Alaa A. Khalaf1; Tariq A. Mandeel1; Nadhem H. Hayder2 | ||
| 1Department of Chemistry- College of science - University Anbar. | ||
| 2Department of Biotechnology-College of Science - Baghdad University | ||
| Abstract | ||
| In this study, the process of separating and analyzing oils from some plant seeds such as Washingtonia tree and Silybum marianum(kulgan) Soxhlat apparatus was used in the extraction process, where extraction was performed using organic solvents (Hexane and Petroleum ether). Then appreciation the percentage of oil in these plants. It was found that the seeds of the Silybum marianum plant contain a higher percentage of oil than the seeds of Washingtonia tree. Then, the active functional groups found in these oils were identified using the (FT-IR) spectrum. The composition of the fatty acids found in the seeds of these plants was also studied using the technique of gas chromatography (GC). This analysis showed five saturated fatty acids and three unsaturated fatty acids, the percentage of these acids in the Washingtonia tree seeds ranged between 1.2-42.7%, while the percentage of the acids in the kulgan seeds ranged between 3.4-54.5%. Also, some physical and chemical properties of extracted fatty acids such (density, acid value, refractive index, flash point) were measured. | ||
| Keywords | ||
| الاستخلاص; نخلة واشنطونیة; الکلغان; کروماتوغرافیا الغازGas chromatography; الاشعة تحت الحمراء Fourier-transform infrared spectroscopy | ||
| References | ||
|
[1] Hossain ,A.B. and Mekhled, M.A. 2010. Biodiesel fuel production from waste canola cooking oil as sustainable energy and environmental recycling process. Australian Journal of Crop Science, 4(7):543-549.
[2] Shivani, P. Khushbu, P. Faldu, N. Thakkar, V. and Shubramanian, R. 2011. Extraction and analysis of Jatropha curcas L. seed oil. African Journal of Biotechnology, 10(79):18210-18213.
[3] Bart, J.C. Palmeri, N. and Cavallaro, S. 2010. Biodiesel Science and Technology from Soil to Oil. Woodhead Publishing Limited, P.1-858.
[4] Hassan, F. M. Aljbory ,I.F. and Kassim T.I. 2013. An attempt to Stimulate lipids for Biodiesel Production from locally Isolated Microalgae in Iraq. Baghdad Science Journal, 10(1):97-108.
[5] ال فلیح, خولة أحمد.2000 . مدخل الى الکیمیاء الحیاتیة. دار الکتب للطباعة والنشر, جامعة الموصل, الطبعة الثانیة, ص83-85. [6]Murray, R.K. Granner, C.K. Mayes, P.A. and Rodwell, V.W. 2003. Harpers III nstrated Biochemistry. Lange Medical Books, McGraw-Hill, New York, P.206-208.
[7] الحلاوجی, أوس نزار.2014 . تحضیر وقود الدیزل الحیوی من نبات الخردل البری ونبات الکلغان ودراسة مواصفاته. أطروحة دکتوراه, قسم الکیمیاء, کلیة التربیة للعلوم الصرفة, جامعة الموصل, ص17. [8]العنزی, مهند عبدالحسن.2012 . استخلاص الزیوت الثابتة من بذور بعض النباتات. مجلة جامعة بابل. .1105-1099:(3)20. [9] Ramadan, M.F. Mörsel, J.T. 2003. Determination of the lipid classes and fatty acid profile of niger seed (Guizotia abyssinica Cass). Phytochemical Analysis,14(6):366-70.
[10] Betiku, E. and Adepoju, T., 2013. Sorrel (Hibiscus sabdariffa) Seed Oil Extraction Optimization and Quality Characterization. American Chemical Science Journal,3(4):449-458.
[11] Hodel, D. R. Greby, K. Ohara ,L. M. and Ohara, E. T. 2015. Infructescence and Fruit Characteristics of Washingtonia. Palmarbor, (2) PP.1‐7.
[12] Nehdi, I.A. 2011. Characteristics and composition of Washingtonia filifera(Linden ex André) H. Wendl. Seed and Seed oil. Food Chem,126(1):197-202.
[13] Greenlee, H. Abascal, K. Yarnell, E. and Ladas, 2007. Clinical applications of Silybum marianum in oncology. Integer Cancer Ther. 6(2):158-165.
[14] Fraschini, F. Dermartini, G. and Esposti, D. 2002. Pharmacology of silymarin. Journal of Clin Drug Invest. 22 ,PP. 51-65.
[15] سلمان, أسراء صکر. و طه, زهراء رافع . 2011 .تأثیر المستخلصات الخام لأوراق الکلغان على الخط الخلوی السرطانی و الخط الخلوی الطبیعی خارج جسم الحی . مجلة جامعة النهرین,(4)14 :76-67. [16] Ali, M.A. Al-Hattab, T.A. and Al-Hydary, I. A. 2015. Extraction of Date Palm seed oil (phoenix dactylifera) by Soxhlet apparatus. International Journal of Advances in Engineering & Technology. 8( 3): 261-271.
[17] Morrison, W. and Smith, L.M., 1964 . Preparation of fatty acid methyl ester and dimethyl acetates from lipids with boron fluoride-methanol", Journal of Lipid Research, 5:600-608.
[18] Canakci, M. and Gerpen, J., 1999. Biodiesel production via acid catalysis transesterification. ASAE, 45(5):1203-1210. | ||
|
Statistics Article View: 369 PDF Download: 297 |
||