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Synthesis and Characterization of Novel Bidentate Ligand type NO and Its Complexes with (CoII , NiII ,CuII and ZnII). | ||
| Journal of Research Diyala humanity | ||
| Article 1, Volume 0, Issue 32, 2017, Pages 34-45 | ||
| Author | ||
| Leqaa khalid Abdulkarim | ||
| Abstract | ||
| The [2-aminobenzothiazole]was reacted with [2,4,6 triyhydroxy-acetophenon monohydrate] to give a new ligand [2-N-2,4,6-trihydroxyacetophenonyliden benzothiazole] [H3L]. This ligand was reacted with metal ions ( CoII, NiII,CuII and ZnII) in methanol as solvent with ( 1:2 ) metal : ligand ratio to give a series of new complexes with general formula [ M(H2L)2],(where:M= CoII, NiII ,CuIIand, ZnII).All compounds were characterized by spectroscopic methods ( I.R , U.V – vis,HPLC) atomic absorption, along with chloride content and conductivity measurements. According to the data of these measurements we suggested a tetrahedral geometry for (CoII, NiII,CuII, and, ZnII ) complexes. | ||
| Keywords | ||
| New Age Allicand binary; the binary Ekand New Age | ||
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