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Synthesis And Characterization of Novel Functionalized Tetradentate Ligand Type H3NS3 And Its Metal Complexes With Re(V), Ni(II), Cu(II), Cd(II) & Hg(II) | ||
| Engineering and Technology Journal | ||
| Article 1, Volume 28, Issue 1, 2010, Pages 43-53 PDF (264.92 K) | ||
| DOI: 10.30684/etj.28.1.4 | ||
| Authors | ||
| Kanan M. Tawfiq; Mohamad J. Al-Jeboori; Matheel D. Al-Sabti | ||
| Abstract | ||
| This work represents the preparation of the tetradentate ligand H3NS3 (H3L) and its metal complexes with rhenium(V), nickle(II), copper(II), cadmium(II) and mercurry(II) metal ions. The ligand and its complexes were characterized when needed by Infrared, Ultraviolet–visible, HPLC, Mass, 1H nuclear magnetic resonance, and atomic absorption spectroscopic techniques, elemental analysis, and electrical conductivity. The proposed structure for (H3NS3) with Re(V) is square pyramidal, with Ni(II) is distorted square planar, and with the rest of metal ions is distorted tetrahedral | ||
| Keywords | ||
| Tetradentate ligand | ||
|
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