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Synthesis of novel metal complexes of 5-(4-isopropoxyphenyl)-Nphenyl- 1,3,4-thiadiazol-2-amine | ||
| Engineering and Technology Journal | ||
| Article 1, Volume 27, Issue 5, 2009, Pages 891-897 PDF (231.51 K) | ||
| DOI: 10.30684/etj.27.5.4 | ||
| Authors | ||
| Ahmed AbdulAmier Hussain Al-Amiery; Muna A. Shakir; Maysoon Yousif | ||
| Abstract | ||
| New5-(4-isopropoxyphenyl)-N-phenyl-1,3,4-thiadiazol-2-amine have been synthesized in good yield by the reaction of N-phenylhydrazinecarbothioamide with a 4- isopropoxybenzoic acid in phosphorusoxychloride. Cr(III), Co(II), Ni(II),Cu(II),Zn(II) and Cd(II) complexes of 5-(4-isopropoxyphenyl)-N-phenyl-1,3,4-thiadiazol-2-amine have been prepared, and characterized by elemental analysis, FT-IR, and UV/visible spectra moreover determination of molar ratio M:L , determination of metal content M% by flame atomic absorption spectroscopy, molar conductance in DMF. solution and magnetic moments (μeff.). | ||
| Keywords | ||
| phenylhydrazinecarbothioamide; DMF; isopropoxyphenyl; Thiadiazol; complexes | ||
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