S. Magtoof AL-Tamemey, M., A. AL-Dakilley, M., Ala, , J. Mahrath, A., Maeky, H. (2010). Synthesis and Characterization of Some New Spiroazetidine-2- one Derivatives. , 0(37), 135-146.
M. S. Magtoof AL-Tamemey; M. A. AL-Dakilley; Ala; a J. Mahrath; H. Maeky. "Synthesis and Characterization of Some New Spiroazetidine-2- one Derivatives". , 0, 37, 2010, 135-146.
S. Magtoof AL-Tamemey, M., A. AL-Dakilley, M., Ala, , J. Mahrath, A., Maeky, H. (2010). 'Synthesis and Characterization of Some New Spiroazetidine-2- one Derivatives', , 0(37), pp. 135-146.
S. Magtoof AL-Tamemey, M., A. AL-Dakilley, M., Ala, , J. Mahrath, A., Maeky, H. Synthesis and Characterization of Some New Spiroazetidine-2- one Derivatives. , 2010; 0(37): 135-146.

Synthesis and Characterization of Some New Spiroazetidine-2- one Derivatives

Iraqi National Journal Of Chemistry
Article 1, Volume 0, Issue 37, 2014, Pages 135-146
Authors
M. S. Magtoof AL-Tamemey; M. A. AL-Dakilley; ; a J. Mahrath; H. Maeky
Abstract
Abstract
The present work include the synthesis and characterization of spiro azetidin-2-one which achieved and expected to have some biological activity . the first step include the treatment of primary aromatic amine with primary aromatic aldehydes in boiling ethanol to give schiff bases which reacted in the second step with carboxylic acid ( 1,3-dithia-2-carboxylicacid )in the presence of triethylamine with phosphorusoxychloride in dry dichloromethane under nitrogen atmosphere at 0°C. To give spiroazetidin-2- one.The new synthesized compound were identified by melting points and UV,FT. IR, Mass, 1H NMR and 13C NMR spectrum
Keywords
spiro; One; Phosphorusoxychloride; ATM; dithiacarboxylic acid
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