D. J, H., K.R, A., M.L, S. (2009). SYNTHESIS AND STRUCTURAL,SPECTROSCOPIC STUDY OF NOVEL BIDENTATE LIGANDS(1,3,4-THIADIAZOLE DERIVATIVES) AND THEIR COMPLEXES WITH Ni(II), pd(II) and pt(IV). , 0(37), 275-291.
Haidar D. J; Azhar K.R; Sajid M.L. "SYNTHESIS AND STRUCTURAL,SPECTROSCOPIC STUDY OF NOVEL BIDENTATE LIGANDS(1,3,4-THIADIAZOLE DERIVATIVES) AND THEIR COMPLEXES WITH Ni(II), pd(II) and pt(IV)". , 0, 37, 2009, 275-291.
D. J, H., K.R, A., M.L, S. (2009). 'SYNTHESIS AND STRUCTURAL,SPECTROSCOPIC STUDY OF NOVEL BIDENTATE LIGANDS(1,3,4-THIADIAZOLE DERIVATIVES) AND THEIR COMPLEXES WITH Ni(II), pd(II) and pt(IV)', , 0(37), pp. 275-291.
D. J, H., K.R, A., M.L, S. SYNTHESIS AND STRUCTURAL,SPECTROSCOPIC STUDY OF NOVEL BIDENTATE LIGANDS(1,3,4-THIADIAZOLE DERIVATIVES) AND THEIR COMPLEXES WITH Ni(II), pd(II) and pt(IV). , 2009; 0(37): 275-291.

SYNTHESIS AND STRUCTURAL,SPECTROSCOPIC STUDY OF NOVEL BIDENTATE LIGANDS(1,3,4-THIADIAZOLE DERIVATIVES) AND THEIR COMPLEXES WITH Ni(II), pd(II) and pt(IV)

Journal of Research Diyala humanity
Article 1, Volume 0, Issue 37, 2017, Pages 275-291
Authors
Haidar D. J; Azhar K.R; Sajid M.L
Abstract
This work reports the synthesis and characterization of two new ligands
5-(p-phenoxy)-1,3,4-thiadiazole - 2- thioacetic acid(HL) and 5-(p-toluyl)-1,3,4-thiadiazole-2-thioacetic acid(HL-). Also complexes of two new ligands (HL) and (HL-) with Ni(II) , pd(II) and pt(IV) in formulas [Ni(L) 2].2 H2O , [Ni(L-)2].H2O ,[pd(L) 2] , [pd(L-)2],[pt(L)2(H2O)2]Cl2 and [pt(L-)2(H2O)2]Cl2.3H2O were prepared . All compounds have been characterized by spectroscopic methods [FT-IR,UV-VIS, Atomic absorption], microanalysis(C.H.N) along with conductivity measurements and magnetic susceptibility . From the above data, the proposed molecular structure for Ni(II) and pd(II) complexes are tetrahedral and square planar geometry respectively, while pt(IV) complexes are forming octahedral geometry
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