I. Abdullah, A., H. Musa, F., A. Mohammad, H. (2009). Synthesis and Studies of -bis ( Thiolethylsuphide-1, 3, 4- Oxadiazole-2yl) Ethane and it's Complexes with (M (II): Cu, Ni, Co, Hg). , 20(1), 75-89. doi: 10.33899/rjs.2009.41330
Ali I. Abdullah; Falih H. Musa; Hikmat A. Mohammad. "Synthesis and Studies of -bis ( Thiolethylsuphide-1, 3, 4- Oxadiazole-2yl) Ethane and it's Complexes with (M (II): Cu, Ni, Co, Hg)". , 20, 1, 2009, 75-89. doi: 10.33899/rjs.2009.41330
I. Abdullah, A., H. Musa, F., A. Mohammad, H. (2009). 'Synthesis and Studies of -bis ( Thiolethylsuphide-1, 3, 4- Oxadiazole-2yl) Ethane and it's Complexes with (M (II): Cu, Ni, Co, Hg)', , 20(1), pp. 75-89. doi: 10.33899/rjs.2009.41330
I. Abdullah, A., H. Musa, F., A. Mohammad, H. Synthesis and Studies of -bis ( Thiolethylsuphide-1, 3, 4- Oxadiazole-2yl) Ethane and it's Complexes with (M (II): Cu, Ni, Co, Hg). , 2009; 20(1): 75-89. doi: 10.33899/rjs.2009.41330

Synthesis and Studies of -bis ( Thiolethylsuphide-1, 3, 4- Oxadiazole-2yl) Ethane and it's Complexes with (M (II): Cu, Ni, Co, Hg)

Rafidain Journal of Science
Article 8, Volume 20, Issue 1, 2009, Pages 75-89    PDF (0 K)
DOI: 10.33899/rjs.2009.41330
Authors
Ali I. Abdullah; Falih H. Musa; Hikmat A. Mohammad
Abstract
The new ligand -bis ( -thiolethysulphide) -1, 3, 4- oxadiazole-2yl) ethane (BTESOE) was prepared from the reaction of 1-, 2-- bis-( - chloro ethylsulphide)-1,3,4-oxadiazol-2yl) ethane with sodium sulphide in aqueous ethanol solution. The ligand was characterized using IR, UV/Vis, 1H-n.m.r, 13C-n.m.r, mass spectroscopies and molar conductivity. BTESOE was employed to synthesize four complexes with metals (M (II): Cu, Ni, Co and Hg), the complexes were studied using IR, UV/Vis, atomic spectroscopies, molar conductivity and magnetic susceptibilities techniques. The results showed that each of these complexes has an octahedral geometry structures.
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