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Synthesis of Some New Fused Heterocyclic Rings Derived from 3-Benzofuranone | ||
| Rafidain Journal of Science | ||
| Article 9, Volume 17, Issue 7, 2006, Pages 76-85 PDF (0 K) | ||
| DOI: 10.33899/rjs.2006.43670 | ||
| Author | ||
| Mohammad A. Eisa | ||
| Abstract | ||
| In the present work, the synthesis of some new fused heterocyclic rings derived from 3-benzofuranone was achieved. 3-Benzofuranone (1) was prepared by the action of polyphosphoric acid on phenoxyacetic acid. 3-Benzofuranone was treated with benzaldehyde and furfural in alkaline medium to afford 2-arylidene-3-benzofuranone (aurones) (2, 3). The reactions of the synthesized aurones with hydrazine hydrate, phenyl hydrazine, hydroxylamine hydrochloride, acetamide, urea and thiourea gave substituted pyrazoline (4, 5), 3-phenyl pyrazoline (6, 7), isoxazole (8, 9), 2-pyridinone and pyrimidin-2-one(thione) (12-15) respectively fused with 3-benzofuran. The structures of the synthesized compounds were confirmed by IR and physical methods. | ||
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