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Synthesis of Some 2,4-Hexadiyne and their Polymers | ||
| Iraqi National Journal Of Chemistry | ||
| Article 1, Volume 0, Issue 18, 2014, Pages 261-271 | ||
| Author | ||
| Mohammad .S.Al-Ajely | ||
| Abstract | ||
| Abstract Diacetylene monomers 2, 3 and 4 were synthesized using Hay coupling procedure. They subjected to -ray irradiation resulted into polymer formation compound (8) while compounds (3a-c) were unsuccessful towrd topochemical polymerization. The corresponding acid chloride compound (5) was then condensed with diamine affording polyamide 6 and 7. The above symmetrically substituted 1,3-diynes together with their polymers have been characterized by combination of spectral methods IR,1H NMR, C13NMR and are discussed. | ||
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