Hamoad Dawood, A., J. Al-Jeboori, M. (2008). Synthesis and spectral studies of 2,6-diformyl-4- methylphenolsemicarbazone ligand and their binuclear metal complexes. , 4(3), 153-162.
Ashour Hamoad Dawood; Mohamad J. Al-Jeboori. "Synthesis and spectral studies of 2,6-diformyl-4- methylphenolsemicarbazone ligand and their binuclear metal complexes". , 4, 3, 2008, 153-162.
Hamoad Dawood, A., J. Al-Jeboori, M. (2008). 'Synthesis and spectral studies of 2,6-diformyl-4- methylphenolsemicarbazone ligand and their binuclear metal complexes', , 4(3), pp. 153-162.
Hamoad Dawood, A., J. Al-Jeboori, M. Synthesis and spectral studies of 2,6-diformyl-4- methylphenolsemicarbazone ligand and their binuclear metal complexes. , 2008; 4(3): 153-162.

Synthesis and spectral studies of 2,6-diformyl-4- methylphenolsemicarbazone ligand and their binuclear metal complexes

journal of kerbala university
Article 1, Volume 4, Issue 3, 2008, Pages 153-162    PDF (0 K)
Authors
Ashour Hamoad Dawood; Mohamad J. Al-Jeboori
Abstract
A new binuclear complexes of Ni+2, Pd+2, Zn+2, Cd+2 and Hg+2 ions with [H3L] {where H3L= 4-Methyl-2,6-bis(formyl semicarbazone) phenol} type (N2O3). The ligand was prepared from reaction two equivalent of semicarbazide hydrochloride with 2,6-diformyl-p-cresol and then reacted with metal ions to form the title complexes. The precursor, ligand and complexes were characterized by {IR, UV-Vis, 1H, 13C, 1H-13C NMR and mass spectroscopy}, molar conductivity, atomic absorption, the microanalysis of elements (C.H.N) and chlore contain. The spectral studies showed the geometry around the Ni+2 and Pd+2 ions are square planar and the Zn+2, Cd+2 and Hg+2 ions are distorted tetrahedral
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