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Synthesis and Characterization of Some New 1,3,4-Thiadiazol Derivatives | ||
| Iraqi National Journal Of Chemistry | ||
| Article 1, Volume 0, Issue 21, 2014, Pages 94-101 | ||
| Authors | ||
| Ikbal S. Al-Shibani; Nejlaa K. E. Al-Yonis; Amar H. Al-Dujaili | ||
| Abstract | ||
| Abstract Fifteen compounds of 2-amino-5-mercapto-1,3,4-thiadiazole derivatives were synthesized and classified into three groups A, B and C. Group A compounds were prepared by condensation reaction of 2-amino-5-mercapto-1,3,4-thiadiazole with some para substituted benzaldehyde and then reacted with ethyl iodide to give the same group C compounds. Group B compounds were synthesized by the reaction of 2-amino-5-methylthio-1,3,4-thiadiazole with the same aldehyde. While, group C compounds were prepared in reverse method to group A compounds by condensation reaction of 2-amino-5ethylthio-1,3,4-thiadiazole with the same para substituted benzaldehyde. All compounds were characterized by elemental analysis, IR and 1HNMR spectral data. These data were confirmed the structural formula of all synthesized compounds. | ||
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