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Preparation , characterization and molecular models of a ligand derivative of the 1,3,4-thiadiazole and some transition metal complexes | ||
| journal of kerbala university | ||
| Article 1, Volume 5, Issue 2, 2009, Pages 61-73 PDF (0 K) | ||
| Author | ||
| Waleed Muhsen Sarhan | ||
| Abstract | ||
| That thiadiazoles derivative are biologically active as antimicrobial agent(1) . therefore, the derivative of the 1,3,4-thiadiazole has prepared along with series of their metal complexes. The reaction of ligand; 2-amino-5-{[(diethylamino)carbonothioyl]dithio}1,3,4-thiadiazole with Cu(II) , Fe (II) , Ni (II) ions yield the following complexes [Cu(ligand)2Cl2], [Fe(ligand)2(H2O)2]SO4, . [Ni(ligand)2Cl2] . The ligand and their metal complexes were characterized using the appropriate techniques, which included melting point, IR,and UV-visible .According to the data obtained, the structural formula with three dimensions of our complexes were suggested. | ||
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