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Synthesis of Some New Sulfanilamide Derivatives | ||
| Journal of Education and Science | ||
| Article 2, Volume 19, Issue 1, 2007, Pages 9-17 PDF (0 K) | ||
| DOI: 10.33899/edusj.2007.51277 | ||
| Author | ||
| Haiffaa Y. Hussain | ||
| Abstract | ||
| ABSTRACT The synthesis of amino acid hydrazide derivatives (4a-f) has been achieved by condensation of the corresponding amino acid hydrazide [3] (which synthesized from sulfanilamide as starting material) with aldehydes or ketones. Compound [3] is also used as a synthone to obtain 1,3,4-oxadiazole-5-thiole [5], which upon reaction with alkyl halide and aldehyde gave compounds (6,7) and (9a-b) respectively. Compound [5] was also allowed to undergo Mannich reaction to give compounds (8a-b). The structure of the synthesized compounds has been confirmed by physical and spectral methods . | ||
| Keywords | ||
| Acid hydrazide; Amino Acid; Sulfanilamide | ||
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