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Synthesis and characterization of metal complexes clerived from S-phenyl amino -2-(2'-hydroxy phenyl)- 1,3,4-thiadiazole. | ||
| Journal of College of Education | ||
| Article 1, Volume 0, Issue 6, 2017, Pages 223-231 | ||
| Authors | ||
| Abd ul. k.Atia; Ahmed. H.Ismail; ; | ||
| Abstract | ||
| A nerv derivative 5 - phenyl amirro 2 - ( 2' - hydroxy phenyl ) 1,3 ,4- thiadiazoleof the fbrntula (Cl4HllN3SO)was prepared by cyclization of l-phenyl ihiosemicarbazide with 2-Sydroxy benzoic acid in presence of oxo-phsphorous trichtoride .The nerv tigand (L) has beett used as ligand to prepare anutnber of rnetal complexesICr(I I l),Co( I I),Ni( I I ),Zn(I I )andCd(I I )]. All the prepared complexes have been studies and characterized ip the solid state by spectral techliques (lR,Uvvisible, elernental of M% in complexes by F'A'A'S, cletermination of M:L ratio, tirrthermore the studying phl"sical properties like(X*)magnetic sr-rsceptibility via Gouy's nrethod,molar concluctivity(A,,)in di rnethy I sul fbxide(DM SO )' | ||
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