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Preparation and Characterization of Mixed Ligands Metal Complexes Derived from Acetylacetonyl P-Imino Acetophenone and 5-Nitroso8-Hydroxyquinoline With Fe (II), Co (II), Ni (II) and Cu (II) Ions | ||
| Engineering and Technology Journal | ||
| Article 1, Volume 30, Issue 13, 2012, Pages 2295-2302 PDF (179.37 K) | ||
| DOI: 10.30684/etj.30.13.10 | ||
| Author | ||
| Rashed Taleb Rasheed | ||
| Abstract | ||
| The Schiff base ligand (HL) has been prepared by the reaction of Paminoacetophenone with acetylacetone. This ligand reacted with 5-nitroso8- hydroxyquinoline (HQ) and salts of first transition series (M) where M= (Fe(II), Co(II), Ni(II) and Cu(II) ions ) to get mononuclear metal (II) complexes of the type [MLQ(H2O)2] have also been synthesized. The formation of the Schiff base ligand and its complexes have been envisaged from FTIR, UV-VIS, magnetic susceptibility, conductivity and atomic absorption technique studies. These studies confirm an octahedral environment around the metal ion in all our complexes. | ||
| Keywords | ||
| Acetylacetone; nitroso; hydroxyquinoline; aminoacetophenone; Schiff base | ||
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