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Synthesis, Spectroscopic and Biological Studies of some metal ions complexes with 2-hydroxy-N-pyridin-2-yl methyl-acetamide | ||
| journal of kerbala university | ||
| Article 1, Volume 1, Issue 0, 2005, Pages 279-289 PDF (0 K) | ||
| Authors | ||
| Lekaa K. Abdul Karim; Enas H.Ali and; Falih H. Musa | ||
| Abstract | ||
| The ligand 2-Hydroxy-N-pyridin-2-ylmethyl-acetamide(L) has been prepared from reaction of 2-(aminomethyl)pyridin with chloroacetic acid (1:1).It has been characterized by elemental analysis (C,H,N) ,'H,13C-NMR, IR and electronic spectra. The complexes of divalent (Co,Ni,Cu,Zn,Cd and Hg) ions and trivalent(Cr) ion have been synthesized and characterized by IR, electronic spectra, molar conductivity, atomic absorption and molar ratio (Ni2+) complex. The analytical studies for the complexes show; octahedral for (Cr3+),square planar for (Cu2+) and (Co,Ni Zn, Cd and Hg) tetrahedral geometries. The study of biological activity of the ligand (L) and its complexes (Co,Ni,Cu,Cd,Hg) in two deferent concentration (1and5) mg/ml showed various activity toward staphylococcus aureus and E.coli . | ||
| Keywords | ||
| synthesis; aminomethyl pyridin; complexes; biological activity | ||
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