- All Journals
- Al-Qadisiyah University
- Basrah University
- Kirkuk University
- Mosul University
- The Iraqi Borad for Medical Specialization
- University of Anbar
- University of Technology
- Al Mustafa University
- Al-Zahraa University for Women
- Alnoor University
- Kunooz University
- Misan University
- Ninevah University
- Tikrit University
- University of Al-Hamdaniya
- University of Kerbala
Microwave Synthesis of some new compounds 1,3 – Oxazepine – 4 , 7 - dione,derivatives from Schiff bases | ||
| Journal of University of Anbar for Pure Science | ||
| Article 15, Volume 6, Issue 3, 2012, Pages 53-59 PDF (1.1 M) | ||
| Document Type: Research Paper | ||
| DOI: 10.37652/juaps.2012.78443 | ||
| Author | ||
| Abed M. Daher* | ||
| Tikrit University - Pharmacy College. | ||
| Abstract | ||
| The Microwave technique is a new method for synthesis of organic compounds, which take a pure and high percent of products and completed with short time, compared with conventional method (heating method). The prepared Schiff bases allowed to react by Microwave technique which is a new apparatus for synthesis the organic compounds, reacts with Malic anhydride to yield (1, 3, 6, 7) 1,3 – Oxazepine compounds and reacted with phthalic anhydrides to yield (2, 4, 5, 8) 1,3 – Oxazepine compounds. The useful thing in Microwave technique is using without solvent there for it called (dry method). The synthesized compounds were identified using Melting point apparatus, Infrared Spectroscopy. | ||
| Keywords | ||
| Microwave Synthesis; oxazepine; dione; derivatives from Schiff bases | ||
| References | ||
|
1- J. Mex. Chem. Soc. 51, (4), (2007)
2- Abed M. Daher Al-Joubory. Ph.D thesis "Synthesis and Comparative Study of some Heterocyclic Compounds Containing Five and Seven – Membered Rings By Conventional and Microwave Method ( MAOS ) and Evaluate the Biological activity of Some of Them", Tikrit University , Education College Pp. 103 – 105, (2010).
3- R. Huisgen, Angew. Chem. Intenat, Ed., 7, 321, (1968).
4- D. Stuerga , M. Delmotte in Microwaves in Organic synthesis (Ed. A. loupy) Wiley-VCH, Weinheim, pp, 1-34, (2002).
5- C. Gabriel, S. Gabriel, E. H. Grant, B. S. Halsted D. M. P. Mingos, Chem. Soc. Rev. 27, 213-223 (1998).
6- I specific cases magnetic field interaction have also been observed, see: D. V. stass. J. R. wood ward, C. R. Timmel P. J. Hore, K, A, mclanchin Chem. Phys, Lett., 329, 15-22, (2000).
7- Williams and Fleming. Spectroscopic Methods in Organic Chemistry. 2nd Ed. Cambridge College. U.K. (1973). | ||
|
Statistics Article View: 469 PDF Download: 444 |
||