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Synthesis , Characterization of Some Metal Complexes with 1,1`bis–(orthoaminophenylthio)-methane | ||
| Al-Mustansiriyah Journal of Science | ||
| Article 1, Volume 19, Issue 2, 2008, Pages 59-68 | ||
| Author | ||
| Shaymaa H. Naji | ||
| Abstract | ||
| The synthesis of 1,1` bis – (orthoaminophenylthio ) – methan from reaction orthoaminophenyl- thiol with methylene dichloride.The new ligand characterized by IR,NMR and mass spectrum.The complexes with some metal ions ( MII = Co , Ni , Cd , Zn , Hg , Pb ) have been prepared and characterized too.The structural diagnosis were established by i.r , Uv – Visible spectrum , conductivities , atomic absorption , formation constant ( Kf ) and magnetic susceptibility .It was concluded from the analysis that the complexes gave the formula C13 H14 N2S2MX and these are mainly six coordinated types. | ||
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