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Application of Chlordiazepoxide as a Complex with Palladium for the Spectrophotometric Determination of Certain Benzodiazepine Drug | ||
| Al-Mustansiriyah Journal of Science | ||
| Article 1, Volume 19, Issue 3, 2008, Pages 52-58 | ||
| Author | ||
| Jwan A.Abdul Sattar | ||
| Abstract | ||
| The present paper describes simple, accurate, rapid, and precise procedure for the determination of Chlordiazepoxide (CDZ) in pure and pharmaceutical dosage form. The proposed method is based on the chelating complexion of Chlordiazepoxide with Palladium. This can be achieved by adjusting pH to(3.0)by adding hydrochloric acid(0.1N)and keeping the reaction for(15min.).The final react with Palladium showed maximum absorbance at a wavelength(424nm).The calibration curve was linear from(5-120) μg.ml-1.The correlation coefficient was(0.9995);the method is sensitive, with detection limit(0.2)μg.ml-1.The results of analysis were validated statistically and recovery studies. | ||
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