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Synthesis of N –sulfamethoxazolederivative imide on polymeric chain | ||
| Baghdad Science Journal | ||
| Article 1, Volume 11, Issue 4, 2014, Pages 1567-1576 | ||
| Authors | ||
| Tamador A. Mahmood; Amal S. Sadiq; Sameaa J. Khammas Al-Bayati | ||
| Abstract | ||
| The present work involved synthesis of several new N-Sulfamethoxazol derivatives imide on Polymeric chain by two steps. The first stip involved preparation of N- (sub.orunsub benzoyl and sub unsub acetyl) amidyl sub sulfamethoxazole (1-5) by condensation of sulfamethoxazole drug with many substituted acid chloride, then the second step include, preparation new five N-(acrly-N–sub or unsub benzoyl) imidyl substituted sulfamethoxazol(6-10) by reaction of poly acryloyl chloride with the prepared compound (1-5) in first stepin asuitable solvent in the presenceamount triethylamine (Et3N) with heating. The structure confirmations of all polymers wereconfirmed using FT-IR,1H-NMR,13C-NMR and UV spectroscopy. Other physical properties including softeningpoint's, melting point, and solubility of the polymers were also measured. | ||
| Keywords | ||
| Sulfamethoxzole drug; poly acryloyl chloride; polyamides derivatives | ||
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